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Solubility System: 1-Chlorobutane with Water (Original Report)

Variables:
Temperature: 274 K - 296 K
Prepared By:
Ari L. Horvath
Experimental Data:
T (°C)w1 x1 Number
16.24112153325.5
3.06.05011780375.3
12.46.99213616536.9
12.56.59612843569.2
17.97.11513855693.4
19.17.01413659738.2
22.77.33114276833.9
23.07.45814524839

a) Gas-liquid system analysis parameter, from calibration measurements.

Method/Apparatus/Procedure:

A 5 μL 1-chlorobutane sample was injected into a 2.3 dm3 equilibration cell containing distilled water. After the cell was shaken vigorously for about 5 minutes, the homogeneity of the liquid sample was maintained with a magnetic stirrer. Compressed air was passed through the cell and the gas flow was measured with a soap film flowmeter. The 1-chlorobutane content was extracted and analyzed using a dual flame ionization detector gas chromatograph.

Source and Purity of Materials:

(1) Source and purity not given.
(2) distilled.

Estimated Errors

Temperature: ±0.5 K.
Solubility: ±2.1%.

References:

No references.

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